Synchro­tron serv­ices for every­one

We provide a new mode for accessing synchrotron facilities for high-throughput powder diffraction measurements and advanced data analytics.

Methods

1
High-resolution X-ray powder diffraction (HR-XRPD)

XRPD is ideal for identification, refinement, and solution of microcrystalline structures. This technique provides a rapid diagnostic for detecting impurities, quantifying phases, determining molecular-scale and morphological properties of matter, and much more

2
Total scattering (TS)

TS goes beyond typical assessment of diffraction peaks to consider the diffuse inten­sities scattered underneath and in between. These carry further in­for­mation about defects, dis­order, dy­nam­ics, and mor­phol­ogy that underpin functional properties.

3
Pair distribution function (PDF) analysis

The PDF gives an alternative perspective to the total sca­ttering signal by trans­for­ming the data to a spa­tial de­pen­den­ce, allowing pro­per­ties such as bond lengths, correlated motions, and local structural features to be observed directly.

4
Small-angle X-ray scattering (SAXS)

SAXS probes the material over very low spatial frequencies. This allows observations of in­ho­mo­ge­neity or periodicity in the density, which can be particularly useful for identifying microphase segregation or mesoporosity. It also can give information about domain morphology and size, for example, of small nanoparticles, when crystallites are sufficiently dilute.

01

Ordering
Simply let us know how many samples you’d like to measure, which techniques, and any additional services, and we’ll get the process started. A quotation of services will be prepared for your needs.

02

Sample Preparation
Once you have confirmed the order, there are two options. Either we can send you a sample preparation kit containing high-throughput sample holders and you load the samples yourself, or, you can send us the samples directly, and we take care of the rest.

03

Delivery
Regardless of the preparation option chosen above, you just need to send us the samples so that we can run the measurements for you.

04

Measurements
Measurements are performed using a high-throughput setup currently installed at one of the most advanced synchrotron light sources in the world: the European Synchrotron Radiation Facility (ESRF) in Grenoble, France. We ensure the setup consistency and collect background and NIST reference standard measurements by default.

05

Data Provisioning
Once the measurements are complete, we ensure that the data are calibrated and processed correctly, characterize the instrumental profile, and perform data transformations for PDF analysis. Furthermore, any step of the data reduction process can be reprocessed on demand.

06

Analysis (optional)
If requested, we can offer guidance or performance of further data analyses to help you reach your R&D goals.

Capabilities

Ultra-High Throughput

Measure up to several thousand samples in one go to finely test sample parameter spaces
  • transmission geometry
  • 2D information using an area detector
  • automated data reduction
  • statistical analysis of large datasets
Use Cases
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High Resolution

Our setup results in a sharp, symmetric instrumental profile and excellent signal-to-noise ratio for improved sensitivity to minute phases and microstructural properties.

  • phase ID
  • Rietveld refinement / quantification
  • indexing / structure solution
Use Cases
LaB6 HighResolution Debye Scherrer Rings

Local Structure

Observe and quantify local structure properties via pair distribution function for nano-, disordered and amorphous materials.
  • local structure refinement
  • coherence length
  • bond coordination environment
Use Cases
LaB6 HighResolution Debye Scherrer Rings

Use Cases

Our services are suitable for both commercial and academic purposes. You can find some examples of different applications with reference to peer-reviewed publications.

Batteries
Understanding ion mobility in next generation batteries
Porous material technologies
Understanding adsorption mechanisms for optimizing materials for gas separation
Mining / Geology
Determination of mineral contents in mining samples
Food Science
Understanding physicochemical behavior in excipient preparations
Food Science
Helping to distinguish melting versus denaturation process of protein structures in high solid confectionaries
Pharmaceuticals
Detecting minority phases/components
Pharmaceuticals
Determining structure-property relationships in amorphous solid formulations
Ion Separators
Determining mechanism of ion loading for ion separation related to nuclear waste remediation

Learn more about our services